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133331-77-8

  • Product Name1-(PERFLUOROHEXYL)OCTANE
  • Molecular FormulaC14H17 F13
  • Molecular Weight432.268
  • Purity99%
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Product Details

Quick Details

  • CasNo: 133331-77-8
  • Molecular Formula: C14H17 F13
  • Purity: 99%

Buy High Purity 1-(PERFLUOROHEXYL)OCTANE 133331-77-8 Factory Supply with Low Price

  • Molecular Formula:C14H17F13
  • Molecular Weight:432.268
  • Vapor Pressure:3.857Pa at 25℃ 
  • Melting Point:4.96 °C 
  • Boiling Point:340 °C 
  • PSA:0.00000 
  • Density:1.331 g/cm3(Temp: 25 °C) 
  • LogP:7.47580 

133331-77-8 Relevant articles

METHOD FOR PRODUCING FLUORINATED COMPOUND

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Paragraph 0151; 0152; 0153; 0154-0159; 0160-0162; 0177-0182, (2019/03/14)

This invention solves the problem of pro...

MANUFACTURING METHOD OF FLUOROALKANE

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, (2019/08/12)

PROBLEM TO BE SOLVED: To provide a manuf...

PROCESS FOR THE PREPARATION OF SEMIFLUORINATED ALKANES USING GRIGNARD REAGENTS

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Page/Page column 63-64, (2019/01/07)

The present invention provides a method ...

PROCESS FOR THE PRODUCTION OF SEMIFLUORINATED ALKANES

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Page/Page column 25; 26; 29; 30; 31; 32; 33; 34, (2018/11/26)

The present invention relates to a proce...

133331-77-8 Process route

oct-1-ene
111-66-0,25068-25-1

oct-1-ene

n-perfluorohexyl iodide
355-43-1

n-perfluorohexyl iodide

1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluoro-8-iodotetradecane
109574-84-7

1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluoro-8-iodotetradecane

1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorotetradecane
133331-77-8

1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorotetradecane

Conditions
Conditions Yield
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; In N,N-dimethyl-formamide; for 12h; Overall yield = 56 %; Irradiation;
 
oct-1-ene
111-66-0,25068-25-1

oct-1-ene

n-perfluorohexyl iodide
355-43-1

n-perfluorohexyl iodide

1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorotetradecane
133331-77-8

1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorotetradecane

Conditions
Conditions Yield
With tris-(trimethylsilyl)silane; oxygen; In water; at 20 ℃; for 36h; Inert atmosphere;
71%
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; In N,N-dimethyl-formamide; for 12h; Irradiation;
45%
Multi-step reaction with 2 steps
1: 1,1,2,2-tetrafluoroethyl-2,2,2-trifluoroethyl ether; diisopropyl peroxydicarbonate / 88 - 100 °C / Large scale
2: palladium 10% on activated carbon; sodium acetate; hydrogen / methanol / Large scale
With diisopropyl peroxydicarbonate; palladium 10% on activated carbon; 1,1,2,2-tetrafluoroethyl-2,2,2-trifluoroethyl ether; hydrogen; sodium acetate; In methanol;
 

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