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InChI:InChI=1/C9H13F9O3Si/c1-19-22(20-2,21-3)5-4-6(10,11)7(12,13)8(14,15)9(16,17)18/h4-5H2,1-3H3
The present invention relates to a metho...
Four silane coupling agents, (1H,1H,2H,2...

(vinyl)trimethoxylsilane


1-iodo-2,2,3,3,4,4,5,5,5-nonafluorobutane


(1H,1H,2H,2H-nonafluorohexyl)trimethoxysilane
| Conditions | Yield |
|---|---|
|
(vinyl)trimethoxylsilane; 1-iodo-2,2,3,3,4,4,5,5,5-nonafluorobutane; With 2,2'-azobis(isobutyronitrile); at 60 ℃; for 6h;
With tri-n-butyl-tin hydride; at 25 ℃; for 4h;
|
75% |

sodium methylate


trichloro(1H,1H,2H,2H-nonafluorohexyl)silane


(1H,1H,2H,2H-nonafluorohexyl)trimethoxysilane
| Conditions | Yield |
|---|---|
|
In methanol; 1,1,2-Trichloro-1,2,2-trifluoroethane; for 1h; Ambient temperature;
|
49.9% |

sodium methylate

trichloro(1H,1H,2H,2H-nonafluorohexyl)silane

3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene

(vinyl)trimethoxylsilane
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