202289-38-1

  • Product NameBis(2-methoxyethyl)aminosulfur trifluoride
  • Molecular FormulaC6H14F3NO2S
  • Molecular Weight221.244
  • Purity99%
  • AppearanceDark yellow-orange liquid
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Product Details

Quick Details

  • CasNo: 202289-38-1
  • Molecular Formula: C6H14F3NO2S
  • Appearance: Dark yellow-orange liquid
  • Purity: 99%

Buy Reliable Quality High Purity Bis(2-methoxyethyl)aminosulfur trifluoride 202289-38-1 Cheapest Price

  • Molecular Formula:C6H14F3NO2S
  • Molecular Weight:221.244
  • Appearance/Colour:Dark yellow-orange liquid 
  • Vapor Pressure:0.0155mmHg at 25°C 
  • Refractive Index:1.392 
  • Boiling Point:256.3 °C at 760 mmHg 
  • PKA:-7.46±0.70(Predicted) 
  • Flash Point:108.8 °C 
  • PSA:47.00000 
  • Density:1.19 g/cm3 
  • LogP:1.95430 

Bis(2-methoxyethyl)aminosulfur trifluoride(Cas 202289-38-1) Usage

Chemical Properties

Dark yellow-orange liquid

Uses

Versatile, thermally stable nucleophilic fluorinating reagent.

InChI:InChI=1/C6H14F3NO2S/c1-11-5-3-10(4-6-12-2)13(7,8)9/h3-6H2,1-2H3

202289-38-1 Relevant articles

Bis(2-methoxyethyl)aminosulfur trifluoride: A new broad-spectrum deoxofluorinating agent with enhanced thermal stability

Lal, Gauri S.,Fez, Guido P.,Pesaresi, Reno J.,Prozonic, Frank M.

, p. 215 - 216 (2007/10/03)

Bis(2-methoxyethyl)aminosulfur trifluori...

Bis(2-methoxyethyl)aminosulfur trifluoride: A new broad-spectrum deoxofluorinating agent with enhanced thermal stability

Lal, Gauri S.,Pez, Guido P.,Pesaresi, Reno J.,Prozonic, Frank M.,Cheng, Hansong

, p. 7048 - 7054 (2007/10/03)

Bis(2-methoxyethyl)aminosulfur trifluori...

202289-38-1 Process route

[bis(2-methoxyethyl)amino]trimethylsilane
221557-49-9

[bis(2-methoxyethyl)amino]trimethylsilane

(bis-(2-methoxyethyl)amino)sulfur trufluoride
202289-38-1

(bis-(2-methoxyethyl)amino)sulfur trufluoride

Conditions
Conditions Yield
With sulfur tetrafluoride; In diethyl ether; at -30 ℃;
70%
In diethyl ether; at -30 - 0 ℃; for 3h;
2.6 g
Bis-(2-methoxyethyl)amine
111-95-5

Bis-(2-methoxyethyl)amine

(bis-(2-methoxyethyl)amino)sulfur trufluoride
202289-38-1

(bis-(2-methoxyethyl)amino)sulfur trufluoride

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1.1: n-BuLi / hexane / -78 - 0 °C
1.2: hexane / 0.5 h / 0 °C
2.1: 2.6 g / diethyl ether / 3 h / -30 - 0 °C
With n-butyllithium; In diethyl ether; hexane; 1.1: Metallation / 1.2: Substitution / 2.1: Substitution;
 

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