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The synthesis of different types of amph...
{2-[2-(3H-imidazol-4-yl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester
β-alanyl-histamine dihydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; In diethyl ether; at 20 ℃; for 2h;
|
71% |
histamine
β-alanyl-histamine dihydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps
1: triethylamine; BOP / CHCl3 / 12 h / 20 °C
2: 71 percent / HCl / diethyl ether / 2 h / 20 °C
With hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In diethyl ether; chloroform;
|
{2-[2-(3H-imidazol-4-yl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester
histamine
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